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Roughness measurement with laser profilometry
Mach, Radoslav ; Frk, Martin (referee) ; Hejátková, Edita (advisor)
The bachelor thesis deals with technology of laser profilometry for material roughness measurements purposes. The theoretical part deals with all aspects of the issue in an effective way and highlights the essential characteristics of used components and material roughness. The focus of this work is in first step to describe the external factors affecting the visual image processing such as increasing of environment temperature and its effect for a camera sensors. And particularly the relationship between CMOS and CCD technologies. The second step is for measuring roughness parameters of materials, such as metal, wood, rubber and plastic with three different lasers. Results demonstrate correlation between the wavelengths of the used laser lights with particular materials.
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Study of optical properties of thin films of perovskiteFAPbBr3 precursors
Smolková, Denisa ; Čech, Vladimír (referee) ; Zmeškal, Oldřich (advisor)
This thesis examines the preparation of thin layers of material for photovoltaic applications with focused on perovskites and determining their optical properties. Basic information about the photovoltaic panels, especially about the perovskites, and the preparation of thin layers is supplied in the theoretical section. This section includes description of optical properties and the main method of study of optical properties, spectroscopic ellipsometry. Experimental section is focused on the preparation of thin layers of perovskites FAPbBr3 and its precursors by spin-coating. Optical properties are evaluated using profilometry, UV VIS spectrometry and spectroscopic ellipsometry. The conclusion summarizes the results of this experiment with focused on comparison of ellipsometric spectrums of perovskites and its precursors.
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Study of electrical and dielectric properties of ionic liquids
Maráčková, Lucie ; Nešpůrek, Stanislav (referee) ; Zmeškal, Oldřich (advisor)
This bachelor´s thesis is focused on a study of electrical and dielectric properties of ionic liquids in the form of solution and thin layers. The values of breakdown voltage have been determined from current-voltage characteristics in solutions. Frequency dependencies have been also observed and used for calculation of values of parallel conductivity and capacity of ionic liquid. It was found that solutions is contained by model with one parallel combination of conductivity and capacity. Thin layers have been created by mixing up PEDOT:PSS with two ionic liquids: 1-butyl-3- methylimidazolium trifluoromethanesulfonate and 1-ethyl-3-methylimidazolium tetrafluoroborate. These layers have created electrochemical battery as is evident from current-voltage characteristics. Frequency dependencies are more complex, a model contained two or respectively three parallel conductivities and capacities which have been influenced by PEDOT:PSS and by ionic liquids characteristics.
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Study of the optical properties of titanium dioxide thin films
Rackovská, Anna Patrícia ; Schmiedová, Veronika (referee) ; Zmeškal, Oldřich (advisor)
The bachelor thesis is focused on the acquirement of thin film layers optical properties characterisation methods, done on inject printed titanium dioxide layers deposed on soda lime glass. Its main emphasis was on spectroscopic ellipsometry that was used to determine the refractive indices and the extinction coefficients of the samples in range of wavelengths from 200 nm to 850 nm and layer thickness. This thesis also shows another options of thin film layers preparation and several other methods to characterise properties of samples, specifically optical microscopy, used to set sample boundary as rough, mechanical profilometry which defined thickness of layers in range of 80 nm for the most thin sample to 250 nm for the most thick sample, and UV-VIS spectroscopy.
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Fabrication of conducting patterns by material electroless plating of printed precursor
Kováčová, Silvia ; Gemeiner,, Pavol (referee) ; Dzik, Petr (advisor)
The subject of this diploma thesis is the preparation of conductive structures by electroless plating of an extruded precursor. The experimental part deals with the preparation of standard patterns based on the length of immersion time in a coppering bath. The precursor layers were applied with Fujifilm Dimatix to various receiver substrates. The individual substrates with the precursor layer were immersed in the copper solution within different time intervals. The structure of the layers of grown copper and their thickness was characterized by a profilometer.
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Study of the optical properties of graphene oxide thin films
Smolková, Denisa ; Zmeškal, Oldřich (referee) ; Schmiedová, Veronika (advisor)
This thesis examines the preparation of thin layers and determining their optical properties. It is focused on graphene oxide. In the theoretical part, basic information about the thin layers and their preparation is supplied. That is followed by a description of various methods of determining their optical properties and properties of light. Experimental part and results are focused on the preparation of thin layers by spin-coating and evaluation of measured values using optical microscopy, profilometry, spectroscopic ellipsometry and UV VIS spectroscopy. The conclusion summarizes the results of these methods.
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Advanced materials for organic bioelectronics
Sedlák, Jiří ; Salyk, Ota (referee) ; Weiter, Martin (advisor)
This bachelor thesis deals with the research of PEDOT:DBSA material for possible use in organic bioelectronics. First, a method for preparing PEDOT:DBSA layers of required thickness was standardized and the dependence of the thickness on the conductivity of the material was monitored. Subsequently, the effect of thermal stabilization and EG, DMSO and H2SO4 substances on the conductivity of prepared layers was tested. Two principles were tested to increase conductivity. The first was the principle of adding substances as dopands into liquid polymeric solutions. The second method of sample preparation was the method of secondary treatment of already prepared layers of pure PEDOT:DBSA. All of prepared polymeric layers were characterize by two methods: four point probe and profilometry.
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Study of optoelectrical properties of organic semiconductor thin film layers of phtalocyanines
Miklíková, Zdeňka ; Vala, Martin (referee) ; Zmeškal, Oldřich (advisor)
Diploma thesis is focused on the study of optoelectric properties of thin layers of organic materials based on phthalocyanines, which can be used as an active layer of photovoltaic cells. Especially are studied the properties of the thin active layers of PdPc and PdPc + IL on the glass or ceramic substrates with aluminium contact, which are prepared by material printing here. On the prepared samples were first measured current-voltage characteristics in the dark and in the light and then were measured impedance spectrums in the dark. The received results will be used to improve the properties and structures of photovoltaic cells.
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Testing of multimodal holographic microscope in reflection mode
Kachtík, Lukáš ; Slabý, Tomáš (referee) ; Křížová, Aneta (advisor)
The thesis is focused on testing of reflection mode of Multimodal holographic microscope constructed in cooperation with TESCAN company. The assessment of axial and lateral resolution, verification of axial intensity response and documentation errors and deficiencies found while measuring are included in the testing procedure. In the conclusion, the Multimodal holographic microscope is compared to an atomic force microscop. A proper understanding of microscope operation and a formulation of an adjustment procedure were essential components of this work.
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Optimization depozition variables during material printing of titania coatings
Mlčkovová, Hana ; Králová, Marcela (referee) ; Dzik, Petr (advisor)
This thesis studies the effect of conditions in the printing material layers of titanium dioxi-de sol-gel formulations for the print properties of the resulting films – TiO2, which were pre-pared from a precursor of titanium tetraisopropoxide (TTIP). Thin films were deposited on the printing material soda lime glass and the layer thickness was controlled by repeatedly apply-ing. Prepared films were subjected to observation under an optical microscope, and the thic-kness of the layers was measured by mechanical profilometry.
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